N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide

Base Information

Chemical Name:N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide
CAS No.:1373404-84-2
Molecular Formula:C₂₄H₄₀N₄O₂S₂
Molecular Weight:480.739
Hs Code.:

Synonyms:N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide

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Chemical Property of N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide

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Technology Process of N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide

There total 2 articles about N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1373405-22-1
C₉H₁₆N₂S

: 423761-68-6
(1S,2S)-N-(2,4,6-trimethylbenzenesulfonyl)-1,2-cyclohexanediamine

: 1373404-84-2
N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1021/ol300798t

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 21436-03-3
(S,S)-1,2-diaminocyclohexane

: 1373404-84-2
N-((1S,2S)-2-(3-((1S,2S)-2-(dimethylamino)cyclohexyl)thioureido)cyclohexyl)-2,4,6-trimethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 20 °C / Cooling with ice

2: dichloromethane / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300798t