bis(1-methyl-2-(p-tolylazo)imidazole)(camphorquinonemonoximato)Ru(II)](ClO₄)

Base Information

• Chemical Name: bis(1-methyl-2-(p-tolylazo)imidazole)(camphorquinonemonoximato)Ru(II)](ClO₄)
• CAS No.: 478495-22-6
• Molecular Formula: C₃₂H₃₈N₉O₂Ru*ClO₄
• Molecular Weight: 781.233

Synonyms:bis(1-methyl-2-(p-tolylazo)imidazole)(camphorquinonemonoximato)Ru(II)](ClO₄)

Chemical Property of bis(1-methyl-2-(p-tolylazo)imidazole)(camphorquinonemonoximato)Ru(II)](ClO₄)

Chemical Property:

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Technology Process of bis(1-methyl-2-(p-tolylazo)imidazole)(camphorquinonemonoximato)Ru(II)](ClO₄)

There total 1 articles about bis(1-methyl-2-(p-tolylazo)imidazole)(camphorquinonemonoximato)Ru(II)](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

cis,trans,cis-(nitro)(nitroso)bis[1-methyl-2-(p-tolylazo)imidazole]ruthenium(II) diperchlorate + camphorquinone monooxime (663-17-2) → bis(1-methyl-2-(p-tolylazo)imidazole)(camphorquinonemonoximato)Ru(II)](ClO4) (478495-22-6)

Guidance literature:

With NaOMe; NaClO₄; In methanol; 1 equiv. of camphorquinone monoxime and NaOMe were added to MeOH soln. of Ru-complex, reflux for 4 h, soln. was cooled and filtered, satd. aq. soln. of NaClO4 was added; the reaction is very slow without NaOMe; soln. was slowly evapd. in air, taking in CH2Cl2, chromy. through silicain toluene, elution with toluene:MeCN=3:1, v/v, evapn. on steam bath, d rying in vac. over P4O10, elem. anal.;

DOI:10.1039/b204442k

upstream raw materials:

camphorquinone monooxime

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