N^α--N^ω-nitro-L-arginine methyl ester

Base Information

Chemical Name:N^α--N^ω-nitro-L-arginine methyl ester
CAS No.:88105-71-9
Molecular Formula:C₃₀H₄₁N₇O₇
Molecular Weight:611.698
Hs Code.:

N<sup>α</sup>-<N-(N-carbobenzoxy-L-prolyl)-DL-2-amino-2-methyl-3-phenylpropyl>-N<sup>ω</sup>-nitro-L-arginine methyl ester

Synonyms:N^α--N^ω-nitro-L-arginine methyl ester

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Chemical Property of N^α--N^ω-nitro-L-arginine methyl ester

Chemical Property:

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Technology Process of N^α--N^ω-nitro-L-arginine methyl ester

There total 4 articles about N^α--N^ω-nitro-L-arginine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 51298-62-5
nitro-L-arginine methyl ester hydrochloride

: 88105-70-8
N-carbobenzoxy-L-prolyl-L-2-amino-2-methyl-1-phenylpropanal

: 88105-71-9
N^α--N^ω-nitro-L-arginine methyl ester

Guidance literature:: With sodium cyanoborohydride; In methanol; at 25 ℃; for 24h;
DOI:10.1021/jm00369a017

Reference yield:

: 21394-84-3
2-amino-2-methyl-3-phenylpropan-1-ol

: 88105-71-9
N^α--N^ω-nitro-L-arginine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / HOBt, DCC / tetrahydrofuran / 2.5 h / 25 °C

2: 67 percent / (COCl)2, DMSO / CH₂Cl₂ / 0.25 h / -60 °C

3: 64 percent / NaCNBH₃ / methanol / 24 h / 25 °C

With oxalyl dichloride; sodium cyanoborohydride; benzotriazol-1-ol; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00369a017

Reference yield:

: 1132-26-9
2-methyl-3-phenylalanine

: 88105-71-9
N^α--N^ω-nitro-L-arginine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / 1 M BH₃ / tetrahydrofuran / 1.) 0 deg C, 4 h, 2.) 25 deg C, 17 h

2: 63 percent / HOBt, DCC / tetrahydrofuran / 2.5 h / 25 °C

3: 67 percent / (COCl)2, DMSO / CH₂Cl₂ / 0.25 h / -60 °C

4: 64 percent / NaCNBH₃ / methanol / 24 h / 25 °C

With oxalyl dichloride; borane; sodium cyanoborohydride; benzotriazol-1-ol; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00369a017