N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANINE-CARBOXY-13C

Base Information

• Chemical Name: N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANINE-CARBOXY-13C
• CAS No.: 84771-22-2
• Molecular Formula: C₁₄H₁₉NO₄
• Molecular Weight: 269.273
• Mol file: 84771-22-2.mol

Synonyms:N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANINE-CARBOXY-13C;N-(tert-butoxycarbonyl)-L-phenylalanine-carboxy-1;N-(TERT-BUTOXYCARBONYL-CARBONYL-13C)-L-P HENYLALANINE, 99 ATOM % 13C;N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANINE- CARBOXY-13C, 99 ATOM % 13C;boc-13c1-phe-oh;boc-phe-oh-1-13c;n-(tert-butoxy(carbonyl-13c1)-l-phenylalanine;n-(tert-butoxycarbonyl)-l-phenylalanine-1-13c

Chemical Property of N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANINE-CARBOXY-13C

Chemical Property:

• Melting Point: 85-87 °C(lit.)
• PSA: 75.63000
• LogP: 2.59790

Purity/Quality:

98% by CP; 99% atom 13C ^*data from raw suppliers

BOC-PHE-OH-1-13C 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANINE-CARBOXY-13C

There total 3 articles about N-(TERT-BUTOXYCARBONYL)-L-PHENYLALANINE-CARBOXY-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + C20(13)C2H29(2)HN(15)NO3S3 → Boc-L-<1,2-(13)C2,2-(2)H,(15)N>Phe (84771-22-2,87713-13-1)

Guidance literature:

Multistep reaction;

DOI:10.1039/cc9960000935

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + (2R,2'S)-N-phenylalanyl>bornane-10,2-sultam → Boc-L-<1,2-13C2,15N>phenylalanine (84771-22-2,87713-13-1)

Guidance literature:

With hydrogenchloride; lithium hydroxide; Yield given. Multistep reaction; 1) THF; 2) THF;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + (2R,2'S)-N-phenylalanyl>bornane-10,2-sultam → Boc-L-<1,2-13C2,3,3-2H2,15N>phenylalanine (84771-22-2,87713-13-1)

Guidance literature:

With hydrogenchloride; lithium hydroxide; Yield given. Multistep reaction; 1) THF; 2) THF;

upstream raw materials:

di-tert-butyl dicarbonate

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