2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside

Base Information

Chemical Name:2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside
CAS No.:1283072-96-7
Molecular Formula:C₂₀H₂₈N₄O₇S
Molecular Weight:468.531
Hs Code.:

Synonyms:2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside

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Chemical Property of 2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside

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Technology Process of 2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside

There total 4 articles about 2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1283072-95-6
2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1283072-96-7
2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 0.5h;
DOI:10.1021/jo102411j

Reference yield:

: 1283072-92-3
4-(4-nitrophenyloxythionocarbonyloxy)-2Z-butenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1283072-96-7
2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / dichloromethane / 20 °C

2: palladium chloride*2MeCN / dichloromethane / 20 h / 40 °C

3: sodium methylate / methanol / 0.5 h / 20 °C

With dmap; palladium chloride*2MeCN; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo102411j

Reference yield:

: 500219-26-1
2-butene-1-ol-4-yl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

: 1283072-96-7
2-[N-(2-azidoethyl)-N-(benzyl)carbamoylthio]-3-butenyl β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; dmap / dichloromethane / 20 °C

2: dmap / dichloromethane / 20 °C

3: palladium chloride*2MeCN / dichloromethane / 20 h / 40 °C

4: sodium methylate / methanol / 0.5 h / 20 °C

With pyridine; dmap; palladium chloride*2MeCN; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo102411j