C₃₁H₃₉FN₄O₇

Base Information

Chemical Name:C₃₁H₃₉FN₄O₇
CAS No.:1353660-65-7
Molecular Formula:C₃₁H₃₉FN₄O₇
Molecular Weight:598.672
Hs Code.:

C<sub>31</sub>H<sub>39</sub>FN<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₁H₃₉FN₄O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₉FN₄O₇

Chemical Property:

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Technology Process of C₃₁H₃₉FN₄O₇

There total 5 articles about C₃₁H₃₉FN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 873326-27-3
(R)-2-((S)-2-((tert-butoxycarbonyl)amino)-N-methyl propanamido)-3-(1H-indol-3-yl)propanoic acid

: 1353660-56-6
(2S,3S)-methyl 3-amino-3-(4-fluorophenyl)-2-methoxypropanoate

: 1353660-65-7
C₃₁H₃₉FN₄O₇

Guidance literature:: With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201101978

Reference yield:

: 174729-15-8
(2S,3R)-methyl 3-(4-fluorophenyl)-2,3-dihydroxypropanoate

: 1353660-65-7
C₃₁H₃₉FN₄O₇

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 23 h / 0 - 20 °C / Inert atmosphere

2: proton sponge / dichloromethane / 20 h / 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 20 °C

4: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With hydrogen azide; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; 1: Mitsunobu reaction;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-38-4
(2S,3S)-methyl 3-azido-3-(4-fluorophenyl)-2-hydroxypropanoate

: 1353660-65-7
C₃₁H₃₉FN₄O₇

Guidance literature:: Multi-step reaction with 3 steps

1: proton sponge / dichloromethane / 20 h / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 20 °C

3: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101978