10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene

Base Information

Chemical Name:10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene
CAS No.:107191-01-5
Molecular Formula:C₂₂H₂₃ClN₂O₃
Molecular Weight:398.889
Hs Code.:

Synonyms:10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene

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Chemical Property of 10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene

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Technology Process of 10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene

There total 2 articles about 10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.6%

: 107191-00-4
2-(5-Chloro-1,4-dihydro-2H-benzo[c][2,7]naphthyridin-3-yl)-1-(3,4-dimethoxy-phenyl)-ethanone

: 107191-01-5
10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene

Guidance literature:: With sodium tetrahydroborate; In ethanol; Ambient temperature;
DOI:10.1248/cpb.34.1901

Reference yield:

: 85732-24-7
1'-(3,4-dimethoxybenzoylmethyl)spiro<4H-3,1-benzoxazine-4,4'-piperidin>-2(1H)-one

: 107191-01-5
10-chloro-2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-2,9-diazaphenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: 40.4 percent / POCl₃ / 5 h / Heating

2: 74.6 percent / NaBH₄ / ethanol / Ambient temperature

With sodium tetrahydroborate; trichlorophosphate; In ethanol;
DOI:10.1248/cpb.34.1901