C₃₃H₅₁BN₂

Base Information

• Chemical Name: C₃₃H₅₁BN₂
• CAS No.: 1192263-61-8
• Molecular Formula: C₃₃H₅₁BN₂
• Molecular Weight: 486.592
• Mol file: 1192263-61-8.mol

Synonyms:C₃₃H₅₁BN₂

Chemical Property of C₃₃H₅₁BN₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₃₃H₅₁BN₂

There total 7 articles about C₃₃H₅₁BN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

triethyl borane (97-94-9) + 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride (250285-32-6) → C33H51BN2 (1192263-61-8)

Guidance literature:

1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

triethyl borane; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol902012c

Reference yield:

1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene*ZnI2*THF + lithium triethylborohydride (22560-16-3) → C33H51BN2 (1192263-61-8)

Guidance literature:

In tetrahydrofuran; at -35 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1071/CH13209

Reference yield:

1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene*GeCl4 + lithium triethylborohydride (22560-16-3) → C33H51BN2 (1192263-61-8) + 1,3-bis(2,6-diisopropylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene (888854-17-9)

Guidance literature:

In tetrahydrofuran; at -35 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1071/CH13209

upstream raw materials:

triethyl borane

1,3-bis[2,6-diisopropylphenyl]imidazolium chloride

lithium triethylborohydride

1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene

Downstream raw materials:

1-ethyl-2-(octyloxymethyl)benzene

cyclohexyl 4-ethylbenzoate

1,1-diphenyl-1-butene