23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin

Base Information

Chemical Name:23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin
CAS No.:1337536-81-8
Molecular Formula:C₄₄H₅₂O₁₇Si
Molecular Weight:880.972
Hs Code.:

Synonyms:23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin

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Technology Process of 23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin

There total 6 articles about 23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: C₆₅H₇₀O₁₇Si

: 1337536-81-8
23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 12h;
DOI:10.1021/jm201034h

Reference yield:

: 160657-48-7
3,5,4-tri(methoxymethyloxy)benzoic acid

: 1337536-81-8
23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 12 h

With dmap; palladium 10% on activated carbon; hydrogen; dicyclohexyl-carbodiimide; In dichloromethane; ethyl acetate;
DOI:10.1021/jm201034h

Reference yield:

: 802918-57-6
silybin

: 1337536-81-8
23-O-tert-butyldimethylsilyl-3-O-[(3',4',5'-tri-O-methoxymethyl)galloyl]silybin

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2: pyridine; silver nitrate / 2 h / 45 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 12 h

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; sodium hydride; silver nitrate; dicyclohexyl-carbodiimide; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm201034h