C₅₈H₆₁N₁₃O₁₃S₆

Base Information

Chemical Name:C₅₈H₆₁N₁₃O₁₃S₆
CAS No.:1160960-62-2
Molecular Formula:C₅₈H₆₁N₁₃O₁₃S₆
Molecular Weight:1340.6
Hs Code.:

C<sub>58</sub>H<sub>61</sub>N<sub>13</sub>O<sub>13</sub>S<sub>6</sub>

Synonyms:C₅₈H₆₁N₁₃O₁₃S₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₈H₆₁N₁₃O₁₃S₆

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Technology Process of C₅₈H₆₁N₁₃O₁₃S₆

There total 4 articles about C₅₈H₆₁N₁₃O₁₃S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4897-84-1
Methyl 4-bromobutyrate

: 960062-15-1
C₅₃H₅₃N₁₃O₁₁S₆

: 1160960-62-2
C₅₈H₆₁N₁₃O₁₃S₆

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 22 ℃; for 48h;

Reference yield:

: C₅₆H₅₄N₁₄O₁₁S₆

: 1160960-62-2
C₅₈H₆₁N₁₃O₁₃S₆

Guidance literature:: Multi-step reaction with 5 steps

1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C

2: triethylamine / acetone / 1 h / Sonication

3: sodium azide / acetone / 1.33 h / 60 °C

4: toluene / 12 h / 75 °C

5: caesium carbonate / N,N-dimethyl-formamide / 48 h / 22 °C

With sodium azide; water; caesium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene; 4: Curtius rearrangement;
DOI:10.1021/jm201685h

Reference yield:

: 1160960-61-1
C₅₁H₄₈N₁₂O₁₁S₆

: 1160960-62-2
C₅₈H₆₁N₁₃O₁₃S₆

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / acetone / 1.33 h / 60 °C

2: toluene / 12 h / 75 °C

3: caesium carbonate / N,N-dimethyl-formamide / 48 h / 22 °C

With sodium azide; caesium carbonate; In N,N-dimethyl-formamide; acetone; toluene; 2: Curtius rearrangement;
DOI:10.1021/jm201685h