(E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate

Base Information

Chemical Name:(E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate
CAS No.:1220520-26-2
Molecular Formula:C₂₇H₃₀O₃
Molecular Weight:402.533
Hs Code.:

Synonyms:(E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate

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Chemical Property of (E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate

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Technology Process of (E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate

There total 1 articles about (E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 3724-55-8
methyl but-3-enoate

: 1220520-21-7
9-[(4-trifluoromethanesulfonyloxyphenyl)(4-hydroxyphenyl)methylene]bicyclo[3.3.1]nonane

: 1220520-26-2
(E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate

Guidance literature:: methyl but-3-enoate; 9-[(4-trifluoromethanesulfonyloxyphenyl)(4-hydroxyphenyl)methylene]bicyclo[3.3.1]nonane; With dichlorobis(triphenylphosphine)palladium; triethylamine; In N,N-dimethyl-formamide; at 20 - 120 ℃; Inert atmosphere;

With hydrogenchloride; In water; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm100047k

Reference yield: 86.0%

: 1220520-26-2
(E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate

: 1220520-30-8
(E)-4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoic acid

Guidance literature:: (E)-methyl 4-[4-[bicyclo[3.3.1]non-9-ylidene(4-hydroxyphenyl)methyl]phenyl]but-3-enoate; With potassium hydroxide; In methanol; at 20 ℃; for 24h;

With hydrogenchloride; In methanol; water;
DOI:10.1021/jm100047k