2-(tetraphen-4-yl)cyclohexanone

Base Information

Chemical Name:2-(tetraphen-4-yl)cyclohexanone
CAS No.:111189-58-3
Molecular Formula:C₂₄H₂₀O
Molecular Weight:324.422
Hs Code.:

Synonyms:2-(4-benzanthracenyl)cyclohexanone

Suppliers and Price of 2-(tetraphen-4-yl)cyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemical Property of 2-(tetraphen-4-yl)cyclohexanone

Chemical Property:

Vapor Pressure:7.02E-13mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(tetraphen-4-yl)cyclohexanone

There total 2 articles about 2-(tetraphen-4-yl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 111189-57-2
2-(4-benz anthracenyl)cyclohexanol

: 111189-58-3
2-(4-benz anthracenyl)cyclohexanone

Guidance literature:: With Dess-Martin periodane; for 0.5h;
DOI:10.1021/jo00235a005

Reference yield:

: 2498-66-0
benz[a]anthracene-7,12-dione

: 111189-58-3
2-(4-benz anthracenyl)cyclohexanone

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / bromine / acetic acid / 4 h / Heating

2: 1.) hydroiodic acid, hypophosphorous acid, 2.) chloranil / 1.) acetic acid, reflux, 18 h, 2.) benzene, reflux, overnight

3: 1.) n-butyllithium / benzene, hexane, 50 deg C, 1 h, 2.) benzene, hexane, 50 deg C, 5 h

4: 85 percent / Dess-Martin reagent / 0.5 h

With n-butyllithium; hydrogen iodide; bromine; hypophosphorous acid; chloranil; Dess-Martin periodane; In acetic acid;
DOI:10.1021/jo00235a005

Reference yield:

: 111189-58-3
2-(4-benz anthracenyl)cyclohexanone

: 206-06-4
Naphtho<2,3b>fluoranthene

Guidance literature:: With PPA; 2,3-dicyano-5,6-dichloro-p-benzoquinone; Yield given. Multistep reaction; 1.) 150 deg C, 4 h, 2.) benzene, reflux 30 min;
DOI:10.1021/jo00235a005