N-(2-methyl-4-heptafluoroisopropylphenyl)-N₂-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide)

Base Information

• Chemical Name: N-(2-methyl-4-heptafluoroisopropylphenyl)-N₂-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide)
• CAS No.: 371771-07-2
• Molecular Formula: C₂₃H₂₃F₇N₂O₃S
• Molecular Weight: 540.502

Synonyms:N-(2-methyl-4-heptafluoroisopropylphenyl)-N₂-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide)

Chemical Property of N-(2-methyl-4-heptafluoroisopropylphenyl)-N₂-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide)

Chemical Property:

Purity/Quality:

99.9% ^*data from raw suppliers

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Technology Process of N-(2-methyl-4-heptafluoroisopropylphenyl)-N₂-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide)

There total 2 articles about N-(2-methyl-4-heptafluoroisopropylphenyl)-N₂-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-4-(heptafluoropropan-2-yl)-aniline (238098-26-5) + N-[1,1-dimethyl-2-(methylthio)ethyl]phthalimide → N-(2-methyl-4-heptafluoroisopropylphenyl)-N2-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide) (371771-07-2)

Guidance literature:

With toluene-4-sulfonic acid; In water; 1,2-dichloro-ethane; at 60 ℃; for 1 - 3h; Product distribution / selectivity;

Reference yield:

N2-[1,1-dimethyl-2-(methylthio)ethyl]-N1-{2-methyl-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl}-1,2-benzenedicarboxamide (371771-01-6) → N-(2-methyl-4-heptafluoroisopropylphenyl)-N2-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide) (371771-07-2)

Guidance literature:

With formic acid; dihydrogen peroxide; In water; 1,2-dichloro-ethane; at 60 ℃; for 1h; Product distribution / selectivity;

Reference yield: 93.3%

N-(2-methyl-4-heptafluoroisopropylphenyl)-N2-(1,1-dimethyl-2-methylsulfonylethyl)-(1,2-benzene formamide) (371771-07-2) → 3-iodo-N1-(2-methyl-4-heptafluoroisopropylphenyl)-N2-(1,1-dimethyl-2-methylsulfonylethyl)-1,2-benzene formamide (272451-69-1,272454-80-5,272454-81-6)

Guidance literature:

With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; palladium on activated charcoal; In N,N-dimethyl-formamide; at 50 ℃; for 3h;

upstream raw materials:

2-methyl-4-(heptafluoropropan-2-yl)-aniline

N₂-[1,1-dimethyl-2-(methylthio)ethyl]-N₁-{2-methyl-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl}-1,2-benzenedicarboxamide

Downstream raw materials:

3-iodo-N₁-(2-methyl-4-heptafluoroisopropylphenyl)-N₂-(1,1-dimethyl-2-methylsulfonylethyl)-1,2-benzene formamide

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