C₂₉H₂₈BrClN₆O

Base Information

• Chemical Name: C₂₉H₂₈BrClN₆O
• CAS No.: 1421322-09-9
• Molecular Formula: C₂₉H₂₈BrClN₆O
• Molecular Weight: 591.938
• Mol file: 1421322-09-9.mol

Synonyms:C₂₉H₂₈BrClN₆O

Chemical Property of C₂₉H₂₈BrClN₆O

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₉H₂₈BrClN₆O

There total 3 articles about C₂₉H₂₈BrClN₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-amino-3,4-dihydro-1H-quinolin-2-one (22246-13-5) → C29H28BrClN6O (1421322-09-9)

Guidance literature:

Multi-step reaction with 4 steps

1: tetraphosphorus decasulfide; triethylamine / acetonitrile

2: cyclohexanol / 6 h / Reflux; Inert atmosphere

3: dichloromethane / 20 °C

4: potassium carbonate / acetone / 10 h / Reflux

With tetraphosphorus decasulfide; potassium carbonate; triethylamine; In dichloromethane; acetone; acetonitrile; cyclohexanol;

DOI:10.1016/j.bmcl.2012.11.078

Reference yield:

C16H13ClN4 (1421321-99-4) → C29H28BrClN6O (1421322-09-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 20 °C

2: potassium carbonate / acetone / 10 h / Reflux

With potassium carbonate; In dichloromethane; acetone;

DOI:10.1016/j.bmcl.2012.11.078

Reference yield:

C18H14Cl2N4O (1421322-01-1) + 1-(2-bromo-benzyl)-piperazine (298705-59-6) → C29H28BrClN6O (1421322-09-9)

Guidance literature:

With potassium carbonate; In acetone; for 10h; Reflux;

DOI:10.1016/j.bmcl.2012.11.078

upstream raw materials:

C₁₈H₁₄Cl₂N₄O

1-(2-bromo-benzyl)-piperazine

6-amino-3,4-dihydro-1H-quinolin-2-one

C₁₆H₁₃ClN₄