CID 6915894

Base Information

• Chemical Name: CID 6915894
• CAS No.: 894-08-6
• Molecular Formula: C18H16 O Pb
• Molecular Weight: 455.524
• DSSTox Substance ID: DTXSID10422592
• Mol file: 894-08-6.mol

Synonyms:CID 6915894;894-08-6;DTXSID10422592;FT-0633086

Chemical Property of CID 6915894

Chemical Property:

• Vapor Pressure: 3.4E-09mmHg at 25°C
• Boiling Point: 458.3°C at 760 mmHg
• Flash Point: 231°C
• PSA: 23.06000
• LogP: 4.24030
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 457.10459
• Heavy Atom Count: 20
• Complexity: 202

Purity/Quality:

98%min ^*data from raw suppliers

LEAD TRIPHENYL HYDROXIDE 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)[Pb](C2=CC=CC=C2)C3=CC=CC=C3.O

Technology Process of CID 6915894

There total 1 articles about CID 6915894 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ triphenylplumbyl hydroxide (894-08-6)

Guidance literature:

A) Hexaphenylblei, 1.) O3, 2.) Hydrolyse;

DOI:10.1016/S0022-328X(00)86330-5

Reference yield: 92.0%

rac-cysteine (921-01-7,3374-22-9,4371-52-2,40143-64-4,40143-66-6,40143-69-9,52-90-4) + triphenylplumbyl hydroxide (894-08-6) → (C6H5)3PbSCH2CH(NH2)COOH

Guidance literature:

In chloroform; water; aminoacid in water was added to the soln. of Pb-compd. in CHCl3 and stirred for 15 min; the organic phase dried with Na2SO4, addn. of petroleum ether, evapn. in vac. at 5°C, the ppt. washed with diethyl ether, dried in vac.;elem. anal.;

Reference yield: 91.0%

triphenylplumbyl hydroxide (894-08-6) + Acetylenedicarboxylic acid (142-45-0) → Acetylen-dicarbonsaeure-bis-triphenylbleisalz (17858-38-7)

Guidance literature:

In methanol; (N2); soln. of metal compd. in dry MeOH was added to MeOH soln. of carboxylic acid (2:1 mol) at room temp. over a period of 15 min and stirred for 1 h; solvent removed in vac.; residue suspd. in warm MeOH, filtered and dried in vac. over silicagel; stored at 0°C in total darkness; elem. anal.;

DOI:10.1002/recl.19881070333

Downstream raw materials:

Pb{OCC(C(CH₃)3)CHC(C(CH₃)3)COCC(C(CH₃)3)CHC(C(CH₃)3)CHCNC}(C₆H₅)3

Acetylen-dicarbonsaeure-bis-triphenylbleisalz

(C₆H₅)3PbSOCC₆H₄COSPb(C₆H₅)3

(t-C₄H₉)2C₆H₂OPb(C₆H₅)3