phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside

Base Information

Chemical Name:phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside
CAS No.:137451-27-5
Molecular Formula:C₃₂H₄₀O₁₇S
Molecular Weight:728.725
Hs Code.:

Synonyms:phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside

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Chemical Property of phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside

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Technology Process of phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside

There total 3 articles about phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 108-98-5
thiophenol

: 14187-83-8
hepta-O-acetyl-α-gentiobiosyl bromide

: 137451-27-5
phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside

Guidance literature:: With sodium carbonate; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1055/s-1991-26559

Reference yield: 75.0%

: 108-98-5
thiophenol

: 4613-78-9
β-D-gentiobiose octaacetate

: 137451-27-5
phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.25h;

Reference yield:

: 74808-10-9
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate

: 124595-24-0
phenyl 2,3,4-tri-O-acetyl-1-thio-β-D-glucopyranoside

: 137451-27-5
phenyl 2,3,4,2',3',4',6'-hepta-O-acetyl-1-thio-β-gentiobioside

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at -45 ℃;
DOI:10.1016/S0040-4039(00)76718-9