(2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

Base Information

Chemical Name:(2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile
CAS No.:1155402-70-2
Molecular Formula:C₁₅H₁₉NO
Molecular Weight:229.322
Hs Code.:

Synonyms:(2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

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Chemical Property of (2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

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Technology Process of (2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

There total 3 articles about (2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 58260-81-4,1155402-76-8
α-ionylideneacetonitrile

: 1155402-70-2
(2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

Guidance literature:: α-ionylideneacetonitrile; With tert.-butylhydroperoxide; potassium carbonate; In water; acetonitrile; at 0 ℃; for 0.5h; Inert atmosphere;

With sodium hypochlorite; In water; acetonitrile; at -5 - 0 ℃; for 8h; Inert atmosphere;
DOI:10.1021/jo900432r

Reference yield: 37.0%

: 58260-81-4,1155402-76-8
α-ionylideneacetonitrile

: 1155402-75-7
(2Z,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

: 1155402-70-2
(2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

Guidance literature:: α-ionylideneacetonitrile; With tert.-butylhydroperoxide; potassium carbonate; In water; acetonitrile; at 0 ℃; for 0.5h; Inert atmosphere;

With sodium hypochlorite; In water; acetonitrile; at -5 - 0 ℃; for 6h; Product distribution / selectivity;

Reference yield:

: 2537-48-6
diethyl 1-cyanomethylphosphonate

: 79734-43-3
3,5,5-trimethyl-4-[(E)-3-oxo-1-butenyl]-2-cyclohexen-1-one

: 1155402-75-7
(2Z,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

: 1155402-70-2
(2E,4E)-3-methyl-5-(2,6,6-trimethyl-4-oxo-2-cyclohexen-1-yl)penta-2,4-dienenitrile

Guidance literature:: diethyl 1-cyanomethylphosphonate; With sodium hydride; In tert-butyl methyl ether; at 5 - 20 ℃; Inert atmosphere;

3,5,5-trimethyl-4-[(E)-3-oxo-1-butenyl]-2-cyclohexen-1-one; In tert-butyl methyl ether; at 0 - 20 ℃;