C₃₂H₃₀N₂O₈

Base Information

Chemical Name:C₃₂H₃₀N₂O₈
CAS No.:1093849-04-7
Molecular Formula:C₃₂H₃₀N₂O₈
Molecular Weight:570.599
Hs Code.:

C<sub>32</sub>H<sub>30</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₃₂H₃₀N₂O₈

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Chemical Property of C₃₂H₃₀N₂O₈

Chemical Property:

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Technology Process of C₃₂H₃₀N₂O₈

There total 11 articles about C₃₂H₃₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093849-02-5
C₁₁H₁₂N₂O₆

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1093849-04-7
C₃₂H₃₀N₂O₈

Guidance literature:: With pyridine;

Reference yield:

: 1093848-92-0
C₂₈H₃₂O₇

: 1093849-04-7
C₃₂H₃₀N₂O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2.1: sulfuric acid / water / 2 h / 20 °C

3.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

3.2: 2 h / Reflux

4.1: potassium carbonate / methanol / 16 h / 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 100 °C

6.1: boron trichloride / dichloromethane / -78 - 0 °C

7.1: 1H-imidazole / N,N-dimethyl-formamide

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane

9.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran

10.1: pyridine

With pyridine; 1H-imidazole; dmap; N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; tetrabutyl ammonium fluoride; water; boron trichloride; potassium carbonate; triethylamine tris(hydrogen fluoride); triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1093848-93-1
C₃₄H₄₆O₇Si

: 1093849-04-7
C₃₂H₃₀N₂O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 16 h / 20 °C

2.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

3.1: sulfuric acid / water / 2 h / 20 °C

4.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

4.2: 2 h / Reflux

5.1: potassium carbonate / methanol / 16 h / 20 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 100 °C

7.1: boron trichloride / dichloromethane / -78 - 0 °C

8.1: 1H-imidazole / N,N-dimethyl-formamide

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane

10.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran

11.1: pyridine

With pyridine; 1H-imidazole; dmap; N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; tetrabutyl ammonium fluoride; water; boron trichloride; potassium carbonate; triethylamine tris(hydrogen fluoride); triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;