C₄₄H₄₄N₄O₄S₃

Base Information

Chemical Name:C₄₄H₄₄N₄O₄S₃
CAS No.:1621326-17-7
Molecular Formula:C₄₄H₄₄N₄O₄S₃
Molecular Weight:789.056
Hs Code.:

C<sub>44</sub>H<sub>44</sub>N<sub>4</sub>O<sub>4</sub>S<sub>3</sub>

Synonyms:C₄₄H₄₄N₄O₄S₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₄₄N₄O₄S₃

Chemical Property:

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Technology Process of C₄₄H₄₄N₄O₄S₃

There total 13 articles about C₄₄H₄₄N₄O₄S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₄₆N₄O₅S₃

: 1621326-17-7
C₄₄H₄₄N₄O₄S₃

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; at 25 ℃; for 24h;
DOI:10.1016/j.bmcl.2014.07.006

Reference yield:

: C₅₉H₅₆N₄O₇S₃

: 1621326-17-7
C₄₄H₄₄N₄O₄S₃

Guidance literature:: Multi-step reaction with 2 steps

1: diethylamine / acetonitrile / 2 h / 25 °C

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 25 °C

With diethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2014.07.006

Reference yield:

: 123226-36-8
3-(bromomethyl)phenylacetonitrile

: 1621326-17-7
C₄₄H₄₄N₄O₄S₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium hydroxide / tetrahydrofuran; water; ethanol / 2 h / 25 °C

2.1: diisobutylaluminium hydride / toluene / 1 h / 0 °C

3.1: N-ethyl-N,N-diisopropylamine; titanium tetrachloride / dichloromethane / 1.08 h / -78 °C

3.2: 1 h / -78 °C

4.1: dmap / dichloromethane / 2 h / 25 °C

5.1: dmap / tetrahydrofuran / 2 h / 0 - 25 °C

6.1: lithium hydroxide / tetrahydrofuran; water / 2 h / 0 °C

7.1: diethylamine / acetonitrile / 2 h / 25 °C

8.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 25 °C

With dmap; titanium tetrachloride; diisobutylaluminium hydride; diethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2014.07.006