(3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione

Base Information

Chemical Name:(3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione
CAS No.:92714-64-2
Molecular Formula:C₁₈H₂₀O₄S
Molecular Weight:332.42
Hs Code.:

Synonyms:(3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione

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Technology Process of (3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione

There total 1 articles about (3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-31-6
maleic anhydride

: (E,E)-4,6-octadienyl phenyl sulfoxide

: 92714-64-2
(3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione

Guidance literature:: In benzene; at 80 ℃; for 24h;
DOI:10.1021/ja00325a017

Reference yield:

: 92714-64-2
(3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione

: (1R,2R,4aS)-7-Benzenesulfinyl-2-methyl-8-oxo-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carboxylic acid

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; -78 deg C, 5 d, -40 deg C, 8 h;
DOI:10.1021/ja00325a017

Reference yield:

: 92714-64-2
(3aR,4R,7S,7aS)-4-(3-Benzenesulfinyl-propyl)-7-methyl-3a,4,7,7a-tetrahydro-isobenzofuran-1,3-dione

: (1R,2R,4aS)-7-Benzenesulfinyl-2-methyl-8-oxo-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1 M lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 deg C, 5 d, -40 deg C, 8 h

With lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/ja00325a017