Technology Process of C14H15F5O2S2
There total 5 articles about C14H15F5O2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; sodium carbonate;
for 5h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: chloroform / 8 h / 0 °C
2.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux
2.2: 0.5 h / Reflux
3.1: water; sodium carbonate / 5 h / Reflux
With
water; sodium methylate; sodium carbonate;
In
tetrahydrofuran; methanol; chloroform;
1.1: |Wittig Olefination;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid; sulfuric acid; sodium nitrite / water / 0.17 h / 0 °C
1.2: 0.5 h / 60 °C
1.3: 1 h / 0 - 30 °C / Inert atmosphere
2.1: triethylamine / tetrahydrofuran / 2 h / 0 °C / Cooling with ice
3.1: chloroform / 8 h / 0 °C
4.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux
4.2: 0.5 h / Reflux
5.1: water; sodium carbonate / 5 h / Reflux
With
sulfuric acid; water; sodium methylate; sodium carbonate; acetic acid; triethylamine; sodium nitrite;
In
tetrahydrofuran; methanol; chloroform; water;
3.1: |Wittig Olefination;