3–phenoxybenzenethiol

Base Information

• Chemical Name: 3–phenoxybenzenethiol
• CAS No.: 92368-12-2
• Molecular Formula: C₁₂H₁₀OS
• Molecular Weight: 202.277
• Mol file: 92368-12-2.mol

Synonyms:3–phenoxybenzenethiol

Chemical Property of 3–phenoxybenzenethiol

Chemical Property:

Purity/Quality:

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Technology Process of 3–phenoxybenzenethiol

There total 6 articles about 3–phenoxybenzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

KS2COEt + 3-phenoxyaniline (3586-12-7) → 3–phenoxybenzenethiol (92368-12-2)

Guidance literature:

With hydrogenchloride; sodium hydroxide; sodium nitrite; In ethanol; water;

Reference yield:

S-3-phenoxyphenyl N,N-dimethylcarbamothioate → 3–phenoxybenzenethiol (92368-12-2)

Guidance literature:

With sodium hydroxide; In methanol; water; at 20 ℃;

DOI:10.1016/j.bioorg.2019.103263

Reference yield:

dithiocarbonic acid O-ethyl ester S-(3-phenoxy-phenyl) ester → 3–phenoxybenzenethiol (92368-12-2)

Guidance literature:

With potassium hydroxide; In ethanol; for 8h; Heating;

DOI:10.1002/jhet.5570370442

upstream raw materials:

3-phenoxyaniline

Downstream raw materials:

5-nitro-4-(3-phenoxy-phenylsulfanyl)-thiophene-2-carboxylic acid methyl ester