1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane

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Chemical Name:1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane
CAS No.:171523-10-7
Molecular Formula:C₄₄H₃₆N₂O₄S₂
Molecular Weight:720.913
Hs Code.:

Synonyms:1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane

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Chemical Property of 1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane

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Technology Process of 1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane

There total 3 articles about 1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 2-<2-(p-tolyl)-1,3-benzoxathiolyl>pyrrole

: 171523-08-3
2-<α-hydroxy-4-methoxybenzyl>-5-<2-(4-methoxyphenyl)-1,3-benzoxathiolyl>pyrrole

: 171523-10-7
1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/0040-4020(95)00704-C

Reference yield:

: 171523-06-1
2,5-bis<2-(4-methoxyphenyl)-1,3-benzoxathiolyl>pyrrole

: 171523-10-7
1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / HgO, 35percent aq. HBF₄ / tetrahydrofuran / Ambient temperature

2: 93 percent / NaBH₄ / methanol; CH₂Cl₂ / 0.5 h / Ambient temperature

3: 53 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

With sodium tetrahydroborate; tetrafluoroboric acid; trifluoroacetic acid; mercury(II) oxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/0040-4020(95)00704-C

Reference yield:

: 171523-07-2
2-(4-methoxybenzoyl)-5-<2-(4-methoxyphenyl)-1,3-benzoxathiolyl>pyrrole

: 171523-10-7
1-<2-(p-tolyl)-1,3-benzoxathiolyl>-5-(p-methoxyphenyl)-9-<2-(p-methoxyphenyl)-1,3-benzoxathiolyl>dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaBH₄ / methanol; CH₂Cl₂ / 0.5 h / Ambient temperature

2: 53 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

With sodium tetrahydroborate; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1016/0040-4020(95)00704-C