tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate

Base Information

Chemical Name:tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate
CAS No.:326496-84-8
Molecular Formula:C₁₉H₃₄O₄Si
Molecular Weight:354.562
Hs Code.:

Synonyms:tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate

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Chemical Property of tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate

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Technology Process of tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate

There total 3 articles about tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 326496-83-7
tert-butyl (2E)-2-((1S,4R,6R)-1-methyl-7-oxa-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-bicyclo[4.1.0]hept-2-ylidene)acetate

: 326496-84-8
tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate

Guidance literature:: With 1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene; In toluene; at 20 - 35 ℃; for 17h;

Reference yield:

: 326496-83-7
tert-butyl (2E)-2-((1S,4R,6R)-1-methyl-7-oxa-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-bicyclo[4.1.0]hept-2-ylidene)acetate

: [5-(tert-butyl-dimethyl-silanyloxy)-2-methyl-3-oxo-cyclohex-1-enyl]-acetic acid tert-butyl ester

: 326496-84-8
tert-butyl (2E)-2-[(3R,5R)-5-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-hydroxy-2-methylene-cyclohexylidene]acetate

: C₃₈H₆₈O₈Si₂

Guidance literature:: With 1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene; triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In toluene; at 20 - 35 ℃;
DOI:10.1021/jo015788y