Technology Process of C27H38FN6O9P
There total 15 articles about C27H38FN6O9P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; acetic acid;
at 20 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium ethanolate / 20 °C
2.1: pyridine / 18 h / 0 °C
3.1: sodium iodide; tetra-(n-butyl)ammonium iodide / acetone / Reflux
3.2: 60 °C
4.1: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 18 h / 0 - 20 °C
5.1: dmap / dichloromethane / 0 °C
6.1: 15-crown-5 / N,N-dimethyl-formamide / 36 h / 90 °C
7.1: ammonia / methanol / 18 h / 20 °C
8.1: 1-methyl-1H-imidazole / acetonitrile / 18 h / 0 - 20 °C
9.1: water; acetic acid / 18 h / 20 °C
With
pyridine; 1-methyl-1H-imidazole; dmap; N-iodo-succinimide; 15-crown-5; ammonia; water; sodium ethanolate; tetra-(n-butyl)ammonium iodide; acetic acid; triethylamine tris(hydrogen fluoride); sodium iodide;
In
methanol; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 15-crown-5 / N,N-dimethyl-formamide / 36 h / 90 °C
2: ammonia / methanol / 18 h / 20 °C
3: 1-methyl-1H-imidazole / acetonitrile / 18 h / 0 - 20 °C
4: water; acetic acid / 18 h / 20 °C
With
1-methyl-1H-imidazole; 15-crown-5; ammonia; water; acetic acid;
In
methanol; N,N-dimethyl-formamide; acetonitrile;