4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol

Base Information

• Chemical Name: 4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol
• CAS No.: 1374443-34-1
• Molecular Formula: C₁₇H₁₅NOS₂
• Molecular Weight: 313.444
• Mol file: 1374443-34-1.mol

Synonyms:4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol

Chemical Property of 4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol

Chemical Property:

Purity/Quality:

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Technology Process of 4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol

There total 1 articles about 4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 2-[(4-methoxyphenyl)ethynyl]-4-methylaniline (1019842-31-9) → 4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol (1374443-34-1) + 4-(4-methoxybenzylidene)-6-methyl-4H-benzo[d][1,3]thiazine-2-thiol (1374443-33-0)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; silver nitrate; In N,N-dimethyl-formamide; at 20 ℃; optical yield given as %de; regiospecific reaction; Inert atmosphere;

DOI:10.1016/j.tet.2012.03.098

upstream raw materials:

carbon disulfide

2-[(4-methoxyphenyl)ethynyl]-4-methylaniline