((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO

Base Information

Chemical Name:((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO
CAS No.:82840-54-8
Molecular Formula:C₃₀H₃₀NiO₂P₂
Molecular Weight:543.205
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)NiCH(CH<sub>3</sub>)CH<sub>2</sub>COO

Synonyms:((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO

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Chemical Property of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO

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Technology Process of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO

There total 3 articles about ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 82840-52-6
(1,2-bis(diphenylphosphino)ethane)NiCH₂CH₂CH₂COO

: 82840-54-8
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO

Guidance literature:: In methanol;
DOI:10.1246/cl.1982.695

Reference yield: 43.0%

: (2,2'-bipyridine)Ni(II)((CH₂)3COO)

: 82840-54-8
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO

Guidance literature:: With 1,2-bis-(diphenylphosphino)ethane; In dichloromethane; under N2 or Ar, CH2Cl2 soln. of nickel complex and dppe stirred at room temp. until color changed from red to yellow; filtered, dried under reduced pressure, solid washed with Et2O, dried; elem. anal.;
DOI:10.1246/bcsj.57.2741

Reference yield:

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 4100-80-5
2-methylsuccinic anhydride

: 15793-01-8
Ni(CO)2{1,2-bis(diphenylphosphino)ethane}

: ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH₂CH(CH₃)COO

: 82840-54-8
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)NiCH(CH₃)CH₂COO

Guidance literature:: With tributylphosphine; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; under N2 or Ar, Schlenk tube contg. THF soln. of reagents placed in thermostated water bath (10°C), P(n-Bu)3 (P(n-Bu)3/Ni=4) added to soln., after 1 h dpe added; solvent removed under reduced pressure, residue washed with hexane;
DOI:10.1246/bcsj.57.2741