C₄₆H₇₀N₄O₉Si

Base Information

Chemical Name:C₄₆H₇₀N₄O₉Si
CAS No.:1428850-31-0
Molecular Formula:C₄₆H₇₀N₄O₉Si
Molecular Weight:851.169
Hs Code.:

C<sub>46</sub>H<sub>70</sub>N<sub>4</sub>O<sub>9</sub>Si

Synonyms:C₄₆H₇₀N₄O₉Si

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Chemical Property of C₄₆H₇₀N₄O₉Si

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Technology Process of C₄₆H₇₀N₄O₉Si

There total 16 articles about C₄₆H₇₀N₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1428850-30-9
C₂₄H₃₄N₂O₂Si

: 1428850-06-9
C₂₂H₃₈N₂O₈

: 1428850-31-0
C₄₆H₇₀N₄O₉Si

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja401457h

Reference yield:

: C₈H₁₃IO₂

: 1428850-31-0
C₄₆H₇₀N₄O₉Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: diisobutylaluminium hydride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.1: triethylamine; dmap / 0 - 20 °C / Inert atmosphere

3.1: caesium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 24 h / 70 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

6.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tert-butyl alcohol; water / 20 °C / Inert atmosphere

7.1: caesium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

8.1: triethylamine; dmap / 2.5 h / 0 - 20 °C / Inert atmosphere

9.1: 2-methyl-but-2-ene; morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 1.5 h / -5 °C / Inert atmosphere

9.2: Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With morpholine; dmap; sodium chlorite; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; diisobutylaluminium hydride; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja401457h

Reference yield:

: 1428850-12-7
C₂₂H₂₉IOSi

: 1428850-31-0
C₄₆H₇₀N₄O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 24 h / 70 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

4.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tert-butyl alcohol; water / 20 °C / Inert atmosphere

5.1: caesium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

6.1: triethylamine; dmap / 2.5 h / 0 - 20 °C / Inert atmosphere

7.1: 2-methyl-but-2-ene; morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 1.5 h / -5 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With morpholine; dmap; sodium chlorite; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja401457h