1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene

Base Information

Chemical Name:1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene
CAS No.:641627-04-5
Molecular Formula:C₁₉H₁₄N₄O
Molecular Weight:314.346
Hs Code.:

Synonyms:1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene

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Chemical Property of 1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene

Chemical Property:

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Technology Process of 1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene

There total 6 articles about 1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 641627-08-9
C₁₉H₁₄N₂O₃

: 641627-04-5
1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene

Guidance literature:: With hydrazine hydrochloride; sodium acetate; In ethanol; water; for 21h; Heating / reflux;

Reference yield:

: 641627-05-6
1-(5-methyl-3-phenylisoxazol-4-yl)propenone

: 641627-04-5
1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; triethylamine; tris-(o-tolyl)phosphine / palladium diacetate / acetonitrile / Heating / reflux

2: perchloric acid; hydrogen / palladium 10% on activated carbon / ethanol / 2.5 h

3: sodium hydride / tetrahydrofuran / 1.42 h / 0 - 20 °C

4: hydrazine hydrochloride; sodium acetate / ethanol; water / 21 h / Heating / reflux

With copper(l) iodide; perchloric acid; hydrazine hydrochloride; hydrogen; sodium acetate; sodium hydride; triethylamine; tris-(o-tolyl)phosphine; palladium 10% on activated carbon; palladium diacetate; In tetrahydrofuran; ethanol; water; acetonitrile;

Reference yield:

: 641627-06-7
3-[3-(5-methyl-3-phenylisoxazol-4-yl)-3-oxo-propenyl]pyridine-2-carboxylic acid methyl ester

: 641627-04-5
1-(5-methyl-3-phenylisoxazol-4-yl)-2,8-dihydro-2,3,4-triaza-cyclopenta[a]indene

Guidance literature:: Multi-step reaction with 3 steps

1: perchloric acid; hydrogen / palladium 10% on activated carbon / ethanol / 2.5 h

2: sodium hydride / tetrahydrofuran / 1.42 h / 0 - 20 °C

3: hydrazine hydrochloride; sodium acetate / ethanol; water / 21 h / Heating / reflux

With perchloric acid; hydrazine hydrochloride; hydrogen; sodium acetate; sodium hydride; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water;