2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide

Base Information

Chemical Name:2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide
CAS No.:1373344-36-5
Molecular Formula:C₂₆H₄₂N₂O₄S
Molecular Weight:478.696
Hs Code.:

Synonyms:2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide

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Chemical Property of 2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide

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Technology Process of 2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide

There total 7 articles about 2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 39085-59-1
trisylhydrazine

: 1373344-41-2
(2S,4aR,8aS)-2-methoxy-4a-methyloctahydrochromen-5-one

: 1373344-36-5
2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1135/cccc2011039

Reference yield:

: (4aR,8aS)-2-hydroxy-4a-methyloctahydrochromen-5-one

: 1373344-36-5
2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: silver(l) oxide / dichloromethane / 20 °C

2: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

With hydrogenchloride; silver(l) oxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1135/cccc2011039

Reference yield:

: C₁₆H₃₀O₃Si

: 1373344-36-5
2,4,6-triisopropyl-N′-((2S,4S,8S)-2-methoxy-4-methyloctahydro-5H-chromen-5-ylidene)benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; tri-tert-butoxyaluminum hydride / tetrahydrofuran; dichloromethane; acetonitrile / 0.25 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: silver(l) oxide / dichloromethane / 20 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

With hydrogenchloride; copper(l) iodide; tri-tert-butoxyaluminum hydride; silver(l) oxide; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1135/cccc2011039