13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene

Base Information

Chemical Name:13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene
CAS No.:103200-74-4
Molecular Formula:C₂₂H₃₄O₂
Molecular Weight:330.511
Hs Code.:

Synonyms:13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene

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Chemical Property of 13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene

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Technology Process of 13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene

There total 3 articles about 13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-24-7
acetic anhydride

: 103200-73-3
9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatrien-13-ol

: 103200-74-4
13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene

Guidance literature:: In pyridine; at 20 - 25 ℃; for 120h;

Reference yield:

: 51077-54-4
9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11-heptadien-13-one

: 103200-74-4
13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene

Guidance literature:: Multi-step reaction with 3 steps

1: 63.5 percent / calcium / liquid ammonia; diethyl ether / 3 h / -45 - -40 °C

2: 98 percent / hydrogen / Lindlar's catal. (deact. Pd), quinoline / petroleum ether

3: 90 percent / pyridine / 120 h / 20 - 25 °C

With hydrogen; calcium; quinoline; Lindlar's catalyst; In pyridine; diethyl ether; ammonia; Petroleum ether;

Reference yield:

: 103200-77-7
9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11-nonadien-14-yn-13-ol

: 103200-74-4
13-acetoxy-9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11,14-nonatriene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / hydrogen / Lindlar's catal. (deact. Pd), quinoline / petroleum ether

2: 90 percent / pyridine / 120 h / 20 - 25 °C

With hydrogen; quinoline; Lindlar's catalyst; In pyridine; Petroleum ether;