2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate
CAS No.:385842-93-3
Molecular Formula:C₂₄H₂₄Cl₃NO₇
Molecular Weight:544.816
Hs Code.:

Synonyms:2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

Suppliers and Price of 2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

Chemical Property:

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Technology Process of 2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

There total 1 articles about 2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-α/β-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 385842-77-3
O-(2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl)trichloroacetimidate

: 385842-93-3
2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/chem.200800352

Reference yield: 90.0%

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: 385842-93-3
2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

: 1381857-85-7
methyl (2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With iron(III) chloride; In dichloromethane; at -60 - 20 ℃; for 0.666667h; Inert atmosphere; Molecular sieve;
DOI:10.1039/c6ra21859h

Reference yield: 83.0%

: 73415-92-6
allyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

: 385842-93-3
2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

: 1044499-96-8
allyl 2-O-(2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: allyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside; 2-O-acetyl-4,6-O-benzylidene-3-O-benzyl-β-D-glucopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 ℃; for 0.5h;
DOI:10.1002/chem.200800352