benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate

Base Information

Chemical Name:benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate
CAS No.:136516-55-7
Molecular Formula:C₂₆H₂₈NO₅P
Molecular Weight:465.486
Hs Code.:

Synonyms:benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate

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Chemical Property of benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate

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Technology Process of benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate

There total 3 articles about benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 146406-23-7,146406-35-1
benzyl α-(9-fluorenylmethoxycarbonylamino)isopropylphosphinate

: 136516-55-7
benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate

Guidance literature:: With sodium periodate; In 1,4-dioxane; water; for 10h;
DOI:10.1055/s-1992-26344

Reference yield:

: 146406-32-8
(1RS)-1-(N-(9-fluorenylmethoxycarbonyl)amino)-2-methylpropylphosphinic acid

: 136516-55-7
benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DCC, DMAP / CH₂Cl₂ / 24 h / Ambient temperature

2: 98 percent / NaIO₄ / dioxane; H₂O / 10 h

With dmap; sodium periodate; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1055/s-1992-26344

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 136516-55-7
benzyl hydrogen α-(9-fluorenylmethoxycarbonylamino)isopropylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DCC, DMAP / CH₂Cl₂ / 24 h / Ambient temperature

2: 98 percent / NaIO₄ / dioxane; H₂O / 10 h

With dmap; sodium periodate; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1055/s-1992-26344