Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate

Base Information

• Chemical Name: Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate
• CAS No.: 104707-84-8
• Molecular Formula: C₁₈H₁₈N₂O₃
• Molecular Weight: 310.353

Synonyms:Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate

Chemical Property of Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate

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Technology Process of Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate

There total 5 articles about Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Dimethyl N-<1-Benzyl-4,5-dimethylpyrrol-2-yl>aminomethylenemalonate (104707-83-7) → Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate (104707-84-8)

Guidance literature:

In various solvent(s); for 0.266667h; Heating;

Reference yield: 69.0%

Dimethyl N-<1-Benzyl-3-carboxy-4,5-dimethylpyrrol-2-yl>aminomethylenemalonate (104707-81-5) → Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate (104707-84-8)

Guidance literature:

With polyphosphoric esters; at 100 ℃; for 2.5h;

Reference yield: 49.0%

Dimethyl N-<1-Benzyl-3-t-butoxycarbonyl-4,5-dimethylpyrrol-2-yl>aminomethylenemalonate (104707-79-1) → Methyl 1-Benzyl-2,3-dimethyl-4-hydroxypyrrolo<2,3-b>pyridine-5-carboxylate (104707-84-8)

Guidance literature:

With polyphosphoric esters; at 90 - 100 ℃; for 3.5h;

upstream raw materials:

Dimethyl N-<1-Benzyl-4,5-dimethylpyrrol-2-yl>aminomethylenemalonate

Dimethyl N-<1-Benzyl-3-carboxy-4,5-dimethylpyrrol-2-yl>aminomethylenemalonate

Dimethyl N-<1-Benzyl-3-t-butoxycarbonyl-4,5-dimethylpyrrol-2-yl>aminomethylenemalonate

1-Benzyl-2-amino-3-t-butoxycarbonyl-4,5-dimethylpyrrole

Downstream raw materials:

1-Benzyl-2,3-dimethyl-4-methoxypyrrolo<2,3-b>pyridine-5-carboxylic Acid

1-Benzyl-2,3,7-trimethyl-4,7-dihydro-4-oxopyrrolo<2,3-b>pyridine-5-carboxylic Acid

Methyl 1-Benzyl-2,3-dimethyl-4-methoxypyrrolo<2,3-b>pyridine-5-carboxylate

Methyl 1-Benzyl-2,3,7-trimethyl-4,7-dihydro-4-oxopyrrolo<2,3-b>pyridine-5-carboxylate

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