3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt

Base Information

Chemical Name:3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt
CAS No.:1383744-17-9
Molecular Formula:C₁₉H₃₁N₂O₅S*K
Molecular Weight:438.63
Hs Code.:

Synonyms:3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt

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Chemical Property of 3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt

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Technology Process of 3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt

There total 3 articles about 3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 126-83-0
sodium 3-chloro-2-hydroxypropane-sulfonate

: (3-tert-butyl-4-methoxybenzyl)-piperazine dihydrochloride

: 1383744-17-9
3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt

Guidance literature:: (3-tert-butyl-4-methoxybenzyl)-piperazine dihydrochloride; With potassium hydrogencarbonate; In water;

sodium 3-chloro-2-hydroxypropane-sulfonate; With potassium iodide; In water; for 5h; Reflux;

Reference yield:

: 107430-92-2
3-tert-butyl-4-methoxybenzaldehyde

: 1383744-17-9
3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 12 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride / ethanol / 5 h / 20 °C

3.1: potassium hydrogencarbonate / water

3.2: 5 h / Reflux

With hydrogenchloride; sodium tris(acetoxy)borohydride; potassium hydrogencarbonate; acetic acid; In ethanol; dichloromethane; water;

Reference yield:

: 1383744-25-9
N-(tert-butyloxycarbonyl)-N'-(3-tert-butyl-4-methoxybenzyl)-piperazine

: 1383744-17-9
3-(1-(3-tert-butyl-4-methoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid potassium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / ethanol / 5 h / 20 °C

2.1: potassium hydrogencarbonate / water

2.2: 5 h / Reflux

With hydrogenchloride; potassium hydrogencarbonate; In ethanol; water;