2,3-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS)-

Base Information

Chemical Name:2,3-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS)-
CAS No.:84104-87-0
Molecular Formula:C₂₀H₃₀O₂
Molecular Weight:302.457
Hs Code.:
Mol file:84104-87-0.mol

Synonyms:2,3-Phenanthrenediol,4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS-trans)-;Podocarpa-8,11,13-triene-12,13-diol, 14-isopropyl- (7CI);8,11,13-Totaratriene-12,13-diol

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS)-

Chemical Property:

Boiling Point:110 °C (0.08 mmHg)
PSA：40.46000
LogP:5.25140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS)-

There total 23 articles about 2,3-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 51905-93-2
12,13-dimethoxy-14-isopropylpodocarpa-8,11,13-triene

: 84104-87-0
(4aS,10aS)-1,2,3,4,4a,9,10,10a-octahydro-6,7-dihydroxy-8-isopropyl-1,1,1,4a-trimethylphenanthrene

Guidance literature:: With boron tribromide; In dichloromethane;

Reference yield: 81.0%

: 51905-87-4
12-aminototara-8,11,13-trien-13-ol

: 84104-87-0
(4aS,10aS)-1,2,3,4,4a,9,10,10a-octahydro-6,7-dihydroxy-8-isopropyl-1,1,1,4a-trimethylphenanthrene

Guidance literature:: With hydrogenchloride; sodium periodate; In acetic acid; at 20 ℃; for 0.0833333h;
DOI:10.1016/S0968-0896(00)00095-X

Reference yield: 60.0%

: 511-15-9
trans-totarol

: 84104-87-0
(4aS,10aS)-1,2,3,4,4a,9,10,10a-octahydro-6,7-dihydroxy-8-isopropyl-1,1,1,4a-trimethylphenanthrene

Guidance literature:: trans-totarol; With m-chlorobenzoyl peroxide; In dichloromethane; at 20 ℃; for 19h;

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 3h; Further stages.;
DOI:10.1248/cpb.56.287