4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt

Base Information

Chemical Name:4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt
CAS No.:1429347-27-2
Molecular Formula:C₁₉H₂₃NO₄S*H₃N
Molecular Weight:378.492
Hs Code.:

Synonyms:4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt

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Chemical Property of 4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt

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Technology Process of 4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt

There total 2 articles about 4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1429347-54-5
N-(2,4-dimethylphenyl)-N-isobutyl-4-vinylbenzenesulfonamide

: 1429347-27-2
4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt

Guidance literature:: N-(2,4-dimethylphenyl)-N-isobutyl-4-vinylbenzenesulfonamide; With potassium permanganate; magnesium sulfate; In water; acetone; at 2 - 20 ℃; Inert atmosphere;

With ammonia; In methanol;

Reference yield:

: 1429346-28-0
4-bromo-N-(2,4-dimethylphenyl)-N-isobutylbenzenesulfonamide

: 1429347-27-2
4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)benzoic acid ammonia salt

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; caesium carbonate; palladium dichloride / water; tetrahydrofuran / 1.5 h / 140 °C / Microwave irradiation

2: potassium permanganate; magnesium sulfate / water; acetone / 2 - 20 °C / Inert atmosphere

With potassium permanganate; magnesium sulfate; caesium carbonate; triphenylphosphine; palladium dichloride; In tetrahydrofuran; water; acetone;