2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

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Chemical Name:2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester
CAS No.:80667-93-2
Molecular Formula:C₃₃H₂₉Br₂N₃O₁₀S
Molecular Weight:819.481
Hs Code.:

2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Synonyms:2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

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Chemical Property of 2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

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Technology Process of 2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

There total 1 articles about 2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 74063-48-2
2-Phenylsulfonylethylchloroformate (PSEC)

: 73461-48-0
N⁴-benzoyl-O^5'-(2-dibromomethyl-benzoyl)-2'-deoxy-cytidine

: 80667-93-2
2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: In pyridine; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4039(01)81988-2

Reference yield: 98.2%

: 80667-93-2
2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

: 73461-48-0
N⁴-benzoyl-O^5'-(2-dibromomethyl-benzoyl)-2'-deoxy-cytidine

Guidance literature:: With triethylamine; In pyridine; at 20 ℃; for 20h; Product distribution; M-NH₃, aq. dioxan, 20 deg C, 7 min. 0.04M K₂CO₃, aq.dioxane, 20 deg C, 1 min.;
DOI:10.1016/S0040-4039(01)81988-2

Reference yield:

: 80667-93-2
2-Dibromomethyl-benzoic acid (2R,3S,5R)-3-(2-benzenesulfonyl-ethoxycarbonyloxy)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

: Carbonic acid 2-benzenesulfonyl-ethyl ester (2R,3S,5R)-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester

Guidance literature:: With morpholine; 2,4,6-trimethyl-pyridine; silver perchlorate; Yield given. Multistep reaction; 1.) 98percent aq. acetone, 1 h;
DOI:10.1016/S0040-4039(01)81988-2