Technology Process of C36H48N2O4
There total 14 articles about C36H48N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H47NO4;
With
hydroxylamine hydrochloride; sodium acetate;
In
ethanol;
at 25 ℃;
for 3h;
With
pyridine; p-toluenesulfonyl chloride;
at 5 ℃;
for 1h;
With
hydrogenchloride;
In
methanol; water; toluene;
at 60 ℃;
for 16h;
regioselective reaction;
DOI:10.1021/jm900305z
- Guidance literature:
-
C36H48N2O6S;
With
hydrogenchloride;
In
methanol; water;
at 60 ℃;
for 17h;
With
sodium hydrogencarbonate;
In
methanol; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 20 °C
1.2: 48 h / 20 °C
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 0.5 h / 20 °C
3.1: Wilkinson's catalyst / toluene / 0.5 h / 80 °C
4.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 0.5 h / 20 °C
5.1: pyridine / 0.5 h / 20 °C
6.1: hydrogenchloride / methanol; water / 17 h / 60 °C
With
pyridine; hydrogenchloride; hydroxylamine hydrochloride; potassium tert-butylate; sodium acetate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
Wilkinson's catalyst;
In
methanol; ethanol; water; toluene; tert-butyl alcohol;