2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Base Information

Chemical Name:2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone
CAS No.:1415243-33-2
Molecular Formula:C₃₂H₂₆N₆O₈
Molecular Weight:622.594
Hs Code.:

Synonyms:2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Technology Process of 2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

There total 2 articles about 2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 81-30-1
1,4,5,8-naphthalenetetracarboxylic dianhydride

: 102494-87-1
N¹-(2-nitrobenzyl)ethane-1,2-diamine

: 1415243-33-2
2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: In isopropyl alcohol; for 2h; Reflux;
DOI:10.1016/j.ejmech.2012.06.045

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 1415243-33-2
2,7-bis-[2-(2-nitrobenzylamino)ethyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 5 h / Reflux; Dean-Stark

1.2: 4 h / 0 - 20 °C

2.1: isopropyl alcohol / 2 h / Reflux

In isopropyl alcohol; toluene;
DOI:10.1016/j.ejmech.2012.06.045