Technology Process of 2-methyl-4,5,6,7-tetraphenyl-1,3-bis[(triisopropylsilyl)ethynyl]-2H-isoindole
There total 5 articles about 2-methyl-4,5,6,7-tetraphenyl-1,3-bis[(triisopropylsilyl)ethynyl]-2H-isoindole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate;
In
1,4-dioxane;
at 135 ℃;
for 24h;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ol401051d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / Inert atmosphere; Reflux
2: palladium diacetate; cyclohexene / 1,4-dioxane / 14 h / 110 °C / Inert atmosphere; Sealed tube
3: potassium phosphate / 1,4-dioxane / 24 h / 135 °C / Inert atmosphere; Sealed tube
With
potassium phosphate; lithium aluminium tetrahydride; palladium diacetate; cyclohexene;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether;
DOI:10.1021/ol401051d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; silver nitrate / acetone / Inert atmosphere
2: potassium phosphate / 1,4-dioxane / 24 h / 135 °C / Inert atmosphere; Sealed tube
With
potassium phosphate; N-Bromosuccinimide; silver nitrate;
In
1,4-dioxane; acetone;
DOI:10.1021/ol401051d
