C₁₄H₂₀S

Base Information

• Chemical Name: C₁₄H₂₀S
• CAS No.: 1195297-61-0
• Molecular Formula: C₁₄H₂₀S
• Molecular Weight: 220.379
• Mol file: 1195297-61-0.mol

Synonyms:C₁₄H₂₀S

Chemical Property of C₁₄H₂₀S

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₄H₂₀S

There total 1 articles about C₁₄H₂₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-thiocresol (106-45-6) + Cyclohexylmethyl bromide (2550-36-9) → C14H20S (1195297-61-0)

Guidance literature:

With potassium carbonate; Inert atmosphere;

DOI:10.1021/ol300672q

Reference yield:

C14H20S (1195297-61-0) → cyclohexylmethyl alcohol (100-49-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium peroxomonosulfate / methanol; water / 12 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: water; dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; hexane / 0.5 h / 20 °C / Inert atmosphere

With n-butyllithium; potassium peroxomonosulfate; water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; hexane; water;

DOI:10.1021/ol300672q

Reference yield:

C14H20S (1195297-61-0) → 1-((cyclohexylmethyl)sulfonyl)-4-methylbenzene

Guidance literature:

With potassium peroxomonosulfate; In methanol; water; at 0 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol300672q

upstream raw materials:

para-thiocresol

Cyclohexylmethyl bromide

Downstream raw materials:

cyclohexylmethyl alcohol