(E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester

Base Information

Chemical Name:(E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester
CAS No.:184866-90-8
Molecular Formula:C₂₈H₂₈O₈
Molecular Weight:492.526
Hs Code.:

Synonyms:(E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester

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Chemical Property of (E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester

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Technology Process of (E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester

There total 3 articles about (E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 184866-90-8
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / 12 h / Ambient temperature

2: SOCl₂ / 3 h / Heating

3: (4-dimethylamino)pyridine, Et₃N / CH₂Cl₂ / 12 h / Ambient temperature

With pyridine; dmap; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/0957-4166(96)00372-2

Reference yield:

: 27542-85-4
4-acetoxycinnamic acid

: 184866-90-8
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 3 h / Heating

2: (4-dimethylamino)pyridine, Et₃N / CH₂Cl₂ / 12 h / Ambient temperature

With dmap; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/0957-4166(96)00372-2

Reference yield:

: 1072-86-2,1460-57-7,1792-81-0,54383-22-1,57794-08-8,931-17-9
(1R,2R)-trans-1,2-cyclohexanediol

: 53901-95-4,108608-06-6,58523-18-5
p-acetoxycinnamoyl chloride

: 184866-90-8
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (1R,2R)-2-[(E)-3-(4-acetoxy-phenyl)-acryloyloxy]-cyclohexyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 12h; Yield given; Ambient temperature;
DOI:10.1016/0957-4166(96)00372-2