3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Base Information

Chemical Name:3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical
CAS No.:869303-05-9
Molecular Formula:C₁₄H₁₉N₂O
Molecular Weight:231.318
Hs Code.:

Synonyms:3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

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Technology Process of 3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

There total 2 articles about 3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 869303-07-1
3-(3-nitrophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

: 869303-05-9
3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 2h; Heating;
DOI:10.1039/b509865c

Reference yield:

: 128954-25-6
3-bromo-2,2,5,5-tetramethyl-Δ³-pyrrolin-1-oxyl

: 869303-05-9
3-(3-aminophenyl)-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / aq. Ba(OH)2 / PdCl₂(PPh₃)2 / dioxane / 3 h / Heating

2: 35 percent / HCO₂NH₄ / Pd/C / methanol / 2 h / Heating

With barium dihydroxide; ammonium formate; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In 1,4-dioxane; methanol; 2: Ehrenkaufer reduction;
DOI:10.1039/b509865c