dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Base Information

Chemical Name:dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester
CAS No.:864365-15-1
Molecular Formula:C₁₈H₂₆ClNO₃S₂
Molecular Weight:403.994
Hs Code.:

dithiocarbonic acid <i>S</i>-{[<i>tert</i>-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester <i>O</i>-(2,2-dimethyl-propyl) ester

Synonyms:dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

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Chemical Property of dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

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Technology Process of dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

There total 4 articles about dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 864365-14-0
N-tert-butyl-N-[4-(tert-butyl-dimethyl-silanyloxy)-2-chloro-phenyl]-2-chloro-acetamide

: sodium O-neopentyl xanthate salt

: 864365-15-1
dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: In N,N-dimethyl-formamide; at 50 ℃; for 3h;
DOI:10.1021/ol051568l

Reference yield:

: 403478-26-2
4-(tert-butyl-dimethyl-silanyloxy)-2-chloro-phenylamine

: 864365-15-1
dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: BF₃*OEt₂ / cyclohexane / 20 °C

2: 79 percent / N,N-dimethylaniline / CH₂Cl₂ / 20 °C

3: 86 percent / dimethylformamide / 3 h / 50 °C

With boron trifluoride diethyl etherate; N,N-dimethyl-aniline; In dichloromethane; cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/ol051568l

Reference yield:

: 864365-13-9
tert-butyl-[4-(tert-butyl-dimethyl-silanyloxy)-2-chloro-phenyl]-amine

: 864365-15-1
dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / N,N-dimethylaniline / CH₂Cl₂ / 20 °C

2: 86 percent / dimethylformamide / 3 h / 50 °C

With N,N-dimethyl-aniline; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol051568l