8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde

Base Information

Chemical Name:8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde
CAS No.:102254-79-5
Molecular Formula:C₂₅H₁₉NO₂S
Molecular Weight:397.497
Hs Code.:

Synonyms:8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde

Chemical Property:

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Technology Process of 8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde

There total 1 articles about 8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 72856-34-9
5-formyl-2-phenyl-6H-1,3-thiazine

: 525-06-4
diphenyl ketene

: 102254-79-5
8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde

Guidance literature:: In toluene; at 100 ℃;

Reference yield:

: 102254-79-5
8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde

: 97182-00-8
4-ethoxycarbonyl-5-formyl-2-phenyl-6H-1,3-thiazine

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / Heating

2: 65 percent / p-toluenesulfonic acid / benzene / 16 h / Heating

3: 50 percent / toluene / 6 h / 90 °C

4: 50 percent / conc. H₂SO₄ / ethanol / Ambient temperature

5: toluene / Heating

With sulfuric acid; toluene-4-sulfonic acid; In ethanol; toluene; benzene;

Reference yield:

: 102254-79-5
8-Oxo-6,7,7-triphenyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-3-carbaldehyde

: 102254-77-3
(dioxolanne-1,3 yl-2)-5 phenyl-2 6H-thiazine-1,3

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / Heating

2: 65 percent / p-toluenesulfonic acid / benzene / 16 h / Heating

With toluene-4-sulfonic acid; In toluene; benzene;