1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate

Base Information

• Chemical Name: 1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate
• CAS No.: 942590-06-9
• Molecular Formula: C₃₅H₄₁N₃O₅S
• Molecular Weight: 615.794

Synonyms:1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate

Chemical Property of 1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate

Chemical Property:

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Technology Process of 1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate

There total 1 articles about 1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dimethylethyl 5-bromo-1H-benzimidazole-1-carboxylate (942590-05-8) + (4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)boronic acid (942589-87-9) → 1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate (942590-06-9)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 80 ℃; for 4h;

Reference yield:

1,1-dimethylethyl 6-(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)-1H-benzimidazole-1-carboxylate (942590-06-9) → C30H33N3O3S

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

upstream raw materials:

1,1-dimethylethyl 5-bromo-1H-benzimidazole-1-carboxylate

(4-{4-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-[(methyloxy)carbonyl]-2-thienyl}phenyl)boronic acid

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