methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate

Base Information

Chemical Name:methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate
CAS No.:73995-77-4
Molecular Formula:C₂₀H₂₆O₅
Molecular Weight:346.423
Hs Code.:

Synonyms:methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate

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Technology Process of methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate

There total 3 articles about methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 53539-02-9
methyl 3α-hydroxy-2β-(benzyloxymethyl)-4-cyclopentene-1α-acetate

: 78-39-7
Triethyl orthoacetate

: 73995-77-4
methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate

Guidance literature:: With hydroquinone; at 140 ℃; for 12h;
DOI:10.1016/0040-4020(81)80005-1

Reference yield:

: 41787-51-3
3α-hydroxy-2β-(benzyloxymethyl)-4-cyclopentene-1α-acetic acid

: 73995-77-4
methyl 2β-(benzyloxymethyl)-5α-(carboethoxymethyl)-3-cyclopentene-1α-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / K₂CO₃ / acetone / 16 h / 35 °C

2: 57 percent / hydroquinone / 12 h / 140 °C

With potassium carbonate; hydroquinone; In acetone;
DOI:10.1016/0040-4020(81)80005-1