C₁₉H₁₈N₂OS

Base Information

Chemical Name:C₁₉H₁₈N₂OS
CAS No.:1414881-37-0
Molecular Formula:C₁₉H₁₈N₂OS
Molecular Weight:322.431
Hs Code.:

C<sub>19</sub>H<sub>18</sub>N<sub>2</sub>OS

Synonyms:C₁₉H₁₈N₂OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₁₈N₂OS

Chemical Property:

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Technology Process of C₁₉H₁₈N₂OS

There total 9 articles about C₁₉H₁₈N₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1414879-06-3
C₁₀H₁₀N₂S

: 501-52-0
3-Phenylpropionic acid

: 1414881-37-0
C₁₉H₁₈N₂OS

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; at 60 ℃; for 1h;

Reference yield:

: 317-20-4
7-fluoro-1H-indole-2,3-dione

: 1414881-37-0
C₁₉H₁₈N₂OS

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide / water / 0.17 h / 110 °C / Microwave irradiation

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 150 °C

3.1: thionyl chloride / dichloromethane / 2 h / 0 °C / Reflux

3.2: 0.5 h / 20 °C

4.1: trichlorophosphate / 1,4-dioxane / 2 h / Reflux

5.1: nickel; hydrogen / methanol / 20 °C

6.1: triethylamine / dichloromethane / 4 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.5 h / 0 - 20 °C

8.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 1 h / 60 °C

With thionyl chloride; hydrogen; boron tribromide; nickel; sodium hydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 8-fluoroquinoline-2,4-dicarboxylic acid

: 1414881-37-0
C₁₉H₁₈N₂OS

Guidance literature:: Multi-step reaction with 8 steps

1.1: diphenylether / 4 h / 20 - 250 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 150 °C

3.1: thionyl chloride / dichloromethane / 2 h / 0 °C / Reflux

3.2: 0.5 h / 20 °C

4.1: trichlorophosphate / 1,4-dioxane / 2 h / Reflux

5.1: nickel; hydrogen / methanol / 20 °C

6.1: triethylamine / dichloromethane / 4 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.5 h / 0 - 20 °C

8.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 1 h / 60 °C

With thionyl chloride; hydrogen; boron tribromide; nickel; sodium hydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; diphenylether; dichloromethane; N,N-dimethyl-formamide; mineral oil;