methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate

Base Information

• Chemical Name: methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate
• CAS No.: 1157855-28-1
• Molecular Formula: C₁₁H₁₀F₃NO₅
• Molecular Weight: 293.199
• Mol file: 1157855-28-1.mol

Synonyms:methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate

Chemical Property of methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate

Chemical Property:

Purity/Quality:

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Technology Process of methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate

There total 1 articles about methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

3-trifluoromethylnitrobenzene (98-46-4) + methyl chloroformate (79-22-1) → methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate (1157855-28-1)

Guidance literature:

With ammonium chloride; zinc; In tetrahydrofuran; water; at 0 ℃;

DOI:10.1055/s-0028-1087943

Reference yield: 93.0%

methyl N-3-trifluoromethylphenyl-N-(methoxycarbonyloxy)carbamate (1157855-28-1) → methyl N-3-trifluoromethylphenyl-N-hydroxycarbamate (1157855-31-6)

Guidance literature:

With methanol; sodium methylate; at 20 ℃;

DOI:10.1055/s-0028-1087943

upstream raw materials:

3-trifluoromethylnitrobenzene

methyl chloroformate

Downstream raw materials:

methyl N-3-trifluoromethylphenyl-N-hydroxycarbamate